Melinda j duer duer covers solid state nmr spectroscopy in an approachable way, with detailed descriptions of the major solid state nmr experiments illustrating what. Introduction to solidstate nmr spectroscopy by duer. Introduction to solid state nmr spectroscopy is written for undergraduate and graduate students of chemistry, either taking a course in advanced or solid state nuclear magnetic resonance spectroscopy or undertaking research projects where solid state nmr is likely to be a major investigative technique. The term nmr crystallography has only recently come into common usage, and even now causes raised eyebrows within some parts of the diffraction community. Duer, ebook format, from the dymocks online bookstore. The discovery has implications for bone health and design of osteomimetic materials. By covering solid state nmr spectroscopy in a clear, straightforward and approachable way with detailed descriptions of the major solid state nmr experiments focussing on what the experiments do and what they tell the researcher, this book serves as an ideal introduction to the subject. The main structural characterization technique we use to study molecular structure in tissues is solidstate nuclear magnetic resonance nmr spectroscopy. Quadrupolar nmr of ionic conductors, batteries, and other energyrelated materials david l. View insights into collagen triple heix structure by solid. This year, the 58 th rmcmr took place in copper mountain, colorado, with over 60 oral and almost 100 poster presentations in the solid state nmr section.
Melinda duer melinda read natural sciences at emmanuel college and completed her phd thesis on parametric probes of ligand field theory in 1988. With additional coverage of the practical implementation of solid state nmr experiments integrated into the discussion, this book will be essential reading for all those using, or about to use, solid state nmr spectroscopy. Emsley university of southampton southampton uk george a. Structural information from quadrupolar nuclei in solid state nmr. Melinda duer is a lecturer in the department of chemistry, university of cambridge and has worked in the field of solidstate nmr spectroscopy for. It presents the current understanding and applications of solid state nmr with a rigorous but readable approach, making it easy for someone who merely. We use a combination of multinuclear solid state nmr spectroscopy, powder xray diffraction, and first principles electronic structure calculations to propose a quantitative structure for this material, in which citrate anions reside in a hydrated layer, bridging between apatitic layers. The contribution of solidstate nmr spectroscopy to. Dr melinda duer is a senior lecturer in the department of chemistry at the university of cambridge, cambridge, uk. Solid state nmr studies of biopolymers edited by ann e. It presents the current understanding and applications of solid state nmr with a rigorous but readable approach, making it easy for someone who merely wishes to gain an overall impression of the subject without details. The royal society of chemistry 2018 experimental approaches of nmr spectroscopy, methodology and application to life science and materials science the nuclear magnetic resonance society of japan ed. This system consisted of an offtheshelf function generator. Outside nmr, sharon is a big fan of football and in particular, of liverpool fc.
Solid state nmr spectroscopy, by melinda duer 2005 middle level publisher webpage for this bookthis is a good middle level book on a number of ssnmr topics, with a detail level that works well for a 23 year graduate student. Melinda j duer, introduction to solid state nmr spectroscopy, wileyblackwell, 2004. We use 2d and 3d c and 15n nmr to study molecular structure in native tissues and in in vitro. Participants at the uk 850 mhz solidstate nmr facility annual symposium. She is also interested in the application of these methods to a wide range of systems including minerals, zeolites and ceramics. Melinda duer is a lecturer in the department of chemistry, university of cambridge and has worked in the field of solidstate nmr spectroscopy for more than ten years. Awarded for solidstate nmr spectroscopy and computational methods. By identifying the carbon atoms in close proximity to the mineral suface in bone, solid state nmr shows that the vital interface between it and the organic matrix is principally polysaccharide and not protein. In situ characterization of advanced glycation end products ages in collagen and model extracellular matrix by solid state nmr.
Morris university of manchester manchester uk biochemical nmr ann e. Solid state nmr spectroscopy has had a major impact on our understanding of the structure of mineralized tissues, in particular bone. Solid state nmr spectroscopy download ebook pdf, epub. Duer this book is for those familiar with solutionstate nmr who are encountering solidstate nmr for the first time. Professor melinda duer took her first degree in natural sciences, specialising in. Thus, the physicochemical and structural state of collagen fibrils is. By contrast, solidstate nmr spectra are very broad, as the full. Duer university of cambridge cambridge uk bernard c. The rocky mountain conference on magnetic resonance rmcmr is a major international conference for the solid state nmr and epr communities.
Department of chemistry, university of cambridge, lens. Her work focuses on studying the structure and dynamics of healthy and glycated extracellular matrix collagen using solid state nmr spectroscopy. The encyclopedia of magnetic resonance emr is based on the original printed encyclopedia of nuclear magnetic resonance. Solidstate nmr spectroscopy principles and applications. Google scholar 2 d c apperley, r k harris and p hodgkinson, solid state nmr. Nmc and david delpy at the facility opening symposium, from left to right steven brown, stephen wimperis, david delpy, ray dupree, jeremy titman, sharon ashbrook, melinda duer, robin harris, dinu iuga. We use 2d and 3d c and 15n nmr to study molecular structure in native tissues and. This cited by count includes citations to the following articles in scholar. Bryce department of chemistry and centre for catalysis research and. Click download or read online button to get solid state nmr spectroscopy book now.
In solution nmr, spectra consist of a series of very sharp. The ones marked may be different from the article in the profile. Solid state 1h nuclear magnetic resonance nmr spectroscopy has developed into a versatile, highresolution method for elucidating the detailed. In the meantime, you can download the document by clicking the download button above. The power of solid state nmr to give crystallographic information has considerably increased since the cpmas suite of techniques was introduced in 1976. Introduction to solidstate nmr spectroscopy book, 2004. Sorry, this document isnt available for viewing at this time. Solid state nmr spectroscopy this book is for those familiar with solution state nmr who are encountering solid state nmr for the first time. Plus, free twoday shipping for six months when you sign up for amazon prime for students. Bone exemplifies the organicinorganic composite structure inherent in mineralized tissues.
This book is for those familiar with solution state nmr who are encountering solid state nmr for the first time. Using solid state nmr to gain structural insight into the mechanism of diseases involving collagen proteins and collagenous tissues. Download pdf solid state nmr spectroscopy free online. It presents the current understanding and applications of solid state nmr with a rigorous but readable approach, making it easy for someone who merely wishes to. More recently, sharon has developed an interest in the application of firstprinciples calculations of nmr parameters in the solid state. Basic principles and practice, momentum press, 2012. State nmr spectroscopy principles and applications.
Dr melinda duer is a senior lecturer in the department of chemistry at the university of cambridge, cambridge. It presents the current understanding and applications of solidstate nmr with a rigorous but readable approach, making it easy for someone who merely wishes to gain an overall impression of the subject without details. Glycation changes molecular organization and charge distribution in. With additional coverage of the practical implementation of solidstate nmr experiments integrated into the discussion, this book will be essential reading for all those using, or about to use, solidstate nmr spectroscopy. Introduction to solidstate nmr spectroscopy duer, melinda j. The book cover links to the publishers website, however copies of this book are available for a cheaper price on other websites. Since then she has transferred into the field of solidstate nmr spectroscopy as has been working in it for more than 10 years. Introduction to solidstate nmr spectroscopy melinda j. Buy ebook solid state nmr spectroscopy by melinda j. Melinda j duer this book is written for undergraduate and graduate students of chemistry, either taking a course in advanced or solid state nuclear magnetic resonance spectroscopy or. By covering solid state nmr spectroscopy in a clear, straightforward and approachable way with detailed descriptions of the major solid state nmr experiments focussing on what the experiments do and what they tell the researcher, this book.
Introduction to solidstate nmr spectroscopy by melinda j duer and a great selection of related books, art and collectibles available now at. Collagen structurefunction relationships from solidstate. Awarded for solid state nmr spectroscopy and computational methods applied to the elucidation of structure and molecular interactions in calcified tissues about the winner professor melinda duer took her first degree in natural sciences, specialising in chemistry, at the university of cambridge in 1985. The organic component of the extracellular matrix in bone is primarily composed of ordered fibrils of collagen triplehelical molecules, in which the.
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